Emulsion Polymerization Reactor

Emulsion Polymerization Reactor The set-up consists of jacketed type SS reactor fitted with a variable speed agitator and baffles.

Hot water from a digitally controlled water bath is circulated in the jacket using a pump. Metered quantity of nitrogen gas from a cylinder passes through a de-oxygenation column & allowed to enter in the reactor. Air has to be evacuated using a vacuum pump to create vacuum up to 30mm of Hg before passing the nitrogen supply. Initiator from reservoir is supplied to the reactor under pressure. Set-up is complete& self-contained with sampling ports. Experiments Effect of monomer concentration Effect of Initiator concentration. Effect of emulsifier concentration. Effect of RPM on conversion Utilities Required Water supply and drain. Electricity- 1.5kw, Single. Instruments, Laboratory wares and Chemicals required for analysis as per the system adopted. Vacuum Pump High purity N2 gas

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